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The preparation method according to any one of claims 1 to 6, wherein Alloc in the Fmoc-Lys(Alloc)-OH is removed twice with either 5-10 equivalents of morpholine or 5-10 equivalents of phenylsilane, and 0.1-0.3 equivalents of Pd(PPh 3 ) 4 for 10-30 min each time, wherein CH 2 Cl 2 is used as a solvent in the removal

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Perez FA, Elfers C, Yanovski JA, Shoemaker AH, Abuzzahab MJ, Roth CL